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LC method for the analysis of acetylsalicylic acid, caffeine and codeine phosphate in pharmaceutical preparations

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dc.contributor.authorAltun, Mehmet Levent
dc.contributor.authorCeyhan, Timurhan
dc.contributor.authorKartal, Müjgan
dc.contributor.authorAtay, Tuğba
dc.contributor.authorÖzdemir, N.
dc.contributor.buuauthorCevheroğlu, Şemsettin
dc.contributor.departmentTıp Fakültesi
dc.contributor.scopusid6602507499
dc.date.accessioned2021-08-23T08:44:33Z
dc.date.available2021-08-23T08:44:33Z
dc.date.issued2001-04
dc.description.abstractAn accurate, simple, reproducible and sensitive method for the determination of acetylsalicylic acid, caffeine and codeine phosphate has been developed and validated. Acetylsalicylic acid, caffeine and codeine phosphate were separated using a mu Bofidapack C-8 column by isocratic elution with flow rate 1.0 ml/min. The mobile phase composition was 125/125/250/0.5 (v/v) isopropyl alcohol, acetonitrile. water and omicron -phosphoric acid. The samples were detected at 215 nm using photo-diode array detector. The linear range of detection for acetylsalicylic acid, caffeine and codeine phosphate were between 0.40 and 1000, 0.25 and 250, and 0.48 and 96 mug/ml, respectively. The linearity, range, selectivity, system performance parameters, precision, accuracy, and ruggedness for acetylsalicylic acid, caffeine and codeine phosphate were also shown to have acceptable values.
dc.identifier.citationAltun, M. L. vd. (2001). "LC method for the analysis of acetylsalicylic acid, caffeine and codeine phosphate in pharmaceutical preparations". Journal of Pharmaceutical and Biomedical Analysis, 25(1), 93-101.
dc.identifier.doi10.1016/S0731-7085(00)00488-X
dc.identifier.endpage101
dc.identifier.issn0731-7085
dc.identifier.issue1
dc.identifier.pubmed11274862
dc.identifier.scopus2-s2.0-0035076243
dc.identifier.startpage93
dc.identifier.urihttps://doi.org/10.1016/S0731-7085(00)00488-X
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S073170850000488
dc.identifier.urihttp://hdl.handle.net/11452/21519
dc.identifier.volume25
dc.identifier.wos000168112900012
dc.indexed.wosSCIE
dc.language.isoen
dc.publisherElsevier
dc.relation.collaborationSanayi
dc.relation.collaborationYurt içi
dc.relation.journalJournal of Pharmaceutical and Biomedical Analysis
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectAcetylsalicylic acid
dc.subjectCaffeine
dc.subjectCodeine phosphate high-performance liquid chromatography
dc.subjectValidation
dc.subjectPerformance liquid-chromatography
dc.subjectAscorbic-acid
dc.subjectTablets
dc.subjectAspirin
dc.subjectSpectrophotometry
dc.subject.scopusParacetamol; 4-Aminophenol; Glassy Carbon Electrode
dc.subject.wosChemistry, analytical
dc.subject.wosPharmacology & pharmacy
dc.titleLC method for the analysis of acetylsalicylic acid, caffeine and codeine phosphate in pharmaceutical preparations
dc.typeArticle
dc.wos.quartileQ3
dspace.entity.typePublication
local.contributor.departmentTıp Fakültesi
local.indexed.atScopus
local.indexed.atWOS

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