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Holodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures

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dc.contributor.authorAkhbari, Kamran
dc.contributor.authorBeheshti, Saeideh
dc.contributor.authorMorsali, Ali
dc.contributor.authorBüyükgüngör, Orhan
dc.contributor.buuauthorYılmaz, Veysel Turan
dc.contributor.departmentFen Edebiyat Fakültesi
dc.contributor.departmentKimya Bölümü
dc.contributor.orcid0000-0002-2849-3332
dc.contributor.researcheridL-7238-2018
dc.contributor.scopusid7006269202
dc.date.accessioned2022-09-09T13:12:55Z
dc.date.available2022-09-09T13:12:55Z
dc.date.issued2014-09-25
dc.description.abstractA new lead(II) three-dimensional coordination polymer, [Pb-2(mu(3)-ANS)(2)(mu(2)-Cl)(2)(H2O)(2)](n) (1) [ANS(-) = 4-amino-1 -naphthalenesulfonateb has been synthesized and characterized. The single-crystal X-ray data of compound 1 shows only one type of Pb-II ion with coordination number of six, the lead atom has distorted octahedral coordination sphere containing stereo-chemically inactive electron lone pair. The thermal stability of 1 was studied by TG-DTA (Thermo gravimetric and differential thermal analyses). Regular morphology of Pb-2(SO4)O nano-particle was prepared from fine powders of compound 1 by calcination process at 700 degrees C. This nano-structure was characterized by XRD (X-ray powder diffraction) and SEM (Scanning electron microscopy).
dc.description.sponsorshipUniversity of Tehran (01/1/389845)
dc.identifier.citationAkhbari, K. vd. (2014). "Holodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures". Journal of Molecular Structure, 1074, 279-283.
dc.identifier.endpage283
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.scopus2-s2.0-84903744929
dc.identifier.startpage279
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2014.06.004
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S0022286014006000
dc.identifier.urihttp://hdl.handle.net/11452/28619
dc.identifier.volume1074
dc.identifier.wos000340315200035
dc.indexed.scopusScopus
dc.indexed.wosSCIE
dc.language.isoen
dc.publisherElsevier
dc.relation.collaborationYurt içi
dc.relation.collaborationYurt dışı
dc.relation.journalJournal of Molecular Structure
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectLead(II)
dc.subjectCoordination polymer
dc.subjectHolodirected
dc.subjectLead oxide sulfate
dc.subjectNano-particle
dc.subjectDesign
dc.subjectRoom
dc.subjectChemistry
dc.subjectDifferential thermal analysis
dc.subjectLead
dc.subjectLead oxide
dc.subjectNanoparticles
dc.subjectScanning electron microscopy
dc.subjectX ray powder diffraction
dc.subjectCoordination number
dc.subjectCoordination polymers
dc.subjectCoordination sphere
dc.subjectElectron lone pair
dc.subjectHolodirected
dc.subjectOctahedral coordination
dc.subjectPolymeric structures
dc.subjectThermo-gravimetric
dc.subjectPolymers
dc.subject.scopusCoordination Polymer; X-Ray Powder Diffraction; Elemental Analyses
dc.subject.wosChemistry, physical
dc.titleHolodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures
dc.typeArticle
dc.wos.quartileQ3
dspace.entity.typePublication
local.contributor.departmentFen Edebiyat Fakültesi/Kimya Bölümü
local.indexed.atWOS
local.indexed.atScopus

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