Yayın: Preparation of PbS and PbO nanopowders from new Pb(II)(saccharine) coordination polymers
Dosyalar
Tarih
Kurum Yazarları
Yılmaz, Veysel Turan
Yazarlar
Aslanı, Alireza
Musevi, Seyid Javad
Şahin, Ertan
Danışman
Dil
Türü
Yayıncı:
Elsevier
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Özet
Nanopowders and single crystal of new Pb(II) three-dimensional coordination polymer, [Pb(H2O)(mu-OAc)(mu-sac)(n), "PASAC" were synthesized by a sonochemical and branched tube methods (Yilmaz et al., Z. Anorg. Allg. Chem. 629 (2003) 172). The new nano-structures of Pb(II) coordination polymer were characterized by X-ray crystallography analysis, scanning electron microscopy (SEM), X-ray powder diffraction (XRD), surface analysis (BET), and IR spectroscopy. The crystal structure of these compounds consists of three-dimensional polymeric units. The thermal stability of compounds was studied by thermal gravimetric analysis (TGA) and differential thermal analyses (DTA). PbS and PbO nano-structures were obtained by calcinations of the nano-structures of this coordination polymer at 600 degrees C.
Açıklama
Bu çalışma, 24-28, Haziran 2013 tarihlerinde Erzurum[Türkiye]’de düzenlenen 9. Nanoscience and Nanotechnology Conference (NANOTR) Kongresi‘nde bildiri olarak sunulmuştur.
Kaynak:
Anahtar Kelimeler:
Konusu
Coordination polymer, PbO, Nanopowder, PbS, Oxide nanoparticles, Ligands, Crystal-structures, Nanostructures, Complexes, Saccharinate, Units, Zn, Crystal structure, X rays, Differential thermal analysis, X ray powder diffraction, Gravimetric analysis, Thermogravimetric analysis, IV-VI semiconductors, Thermodynamic stability, Lead, Single crystals, Lead oxide, Surface analysis, Nanostructured materials, Scanning electron microscopy, Nanostructures, Polymers, Coordination Polymers, Tube methods, Differential thermal analyses (DTA), Thermal gravimetric analyses (TGA), Dimensional coordinations, Nano powders, Sonochemical, X ray crystallography
Alıntı
Aslani, A. vd. (2014). "Preparation of PbS and PbO nanopowders from new Pb(II)(saccharine) coordination polymers". Applied Surface Science, 318, 206-212.