Syntheses and characterizations of a novel 1,2,3,4-tetrahydroquinazoline and a Co(III) complex

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dc.contributor.authorÇolak, Alper Tolga
dc.contributor.authorYılmaz, Filiz
dc.contributor.buuauthorMutlu, Hasene
dc.contributor.buuauthorİrez, Gazi
dc.contributor.departmentUludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü.tr_TR
dc.contributor.orcid0000-0002-0026-7755tr_TR
dc.contributor.researcheridAAH-2888-2021tr_TR
dc.contributor.scopusid57212275330tr_TR
dc.contributor.scopusid6602755323tr_TR
dc.date.accessioned2022-05-24T11:31:07Z
dc.date.available2022-05-24T11:31:07Z
dc.date.issued2012
dc.description.abstractThe 2-furan-2-yl-1,2,3,4-tetrahydroquinazoline-2-carbaldehyde oxime (HL) and complex of tridentate ligand containing oxime, imine, and amine donors resulting from reactions with cobalt(II) salt have been synthesized and characterized by spectral methods (FT-IR, NMR, UV-Vis, mass), elemental analysis, magnetic susceptibility, molar conductivity, and thermal analysis (TG, DTA) techniques. The molecular structure of HL was elucidated from single-crystal X-ray diffraction. X-ray crystallographic analysis shows that the molecule crystallizes in the monoclinic system, space group C2/c. In the complex, chloride was not coordinated as confirmed by conductivity measurements. The metal is coordinated to the oxime, imine, and amine nitrogen atoms and decomposes with loss of the organic ligand and halogen to leave metal oxide. The metal to ligand ratio was 1 : 2 by elemental analysis and mass spectrum.en_US
dc.identifier.citationMutlu, H. vd. (2012). "Syntheses and characterizations of a novel 1,2,3,4-tetrahydroquinazoline and a Co(III) complex". Journal of Coordination Chemistry, 65(12), 2192-2200.en_US
dc.identifier.endpage2200tr_TR
dc.identifier.issn0095-8972
dc.identifier.issue12tr_TR
dc.identifier.scopus2-s2.0-84861886371tr_TR
dc.identifier.startpage2192tr_TR
dc.identifier.urihttps://doi.org/10.1080/00958972.2012.688823
dc.identifier.urihttps://www.tandfonline.com/doi/full/10.1080/00958972.2012.688823
dc.identifier.urihttp://hdl.handle.net/11452/26659
dc.identifier.volume65tr_TR
dc.identifier.wos000304328900013tr_TR
dc.indexed.scopusScopusen_US
dc.indexed.wosSCIEen_US
dc.language.isoenen_US
dc.publisherTaylor & Francisen_US
dc.relation.bap2006/66tr_TR
dc.relation.collaborationYurt içitr_TR
dc.relation.journalJournal of Coordination Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergitr_TR
dc.relation.tubitak106T371tr_TR
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectChemistryen_US
dc.subject2-furan-2-yl-1,2,3,4-tetrahydroquinazoline-2-carbaldehyde oximeen_US
dc.subjectAmine-imine-oximeen_US
dc.subjectSchiff baseen_US
dc.subjectCobalt(III) complexen_US
dc.subject2-aminobenzyl amineen_US
dc.subjectTransition-metal-complexesen_US
dc.subjectRing-chain tautomerismen_US
dc.subjectSolvent-free synthesisen_US
dc.subjectOxime ligandsen_US
dc.subjectSpectrophotometric determinationen_US
dc.subjectTetravalent nickelen_US
dc.subjectQuinazolinesen_US
dc.subjectChemistryen_US
dc.subjectEfficienten_US
dc.subjectDerivativesen_US
dc.subject.scopusSemicarbazone Derivative; 4-toluenesulfinic Acid; Thionesen_US
dc.subject.wosChemistry, inorganic & nuclearen_US
dc.titleSyntheses and characterizations of a novel 1,2,3,4-tetrahydroquinazoline and a Co(III) complexen_US
dc.typeArticle
dc.wos.quartileQ2en_US

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