Sadeghzadeh, HomaMorsali, AliBüyükgüngör, Orhan2021-12-022021-12-022010-04-15Sadeghzadeh, H. vd. (2010). "Synthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursor". Materials Letters, 64(7), 810-813.0167-577X1873-4979https://doi.org/10.1016/j.matlet.2010.01.017https://www.sciencedirect.com/science/article/pii/S0167577X10000297http://hdl.handle.net/11452/22947A new Pb(II) one-dimensional coordination polymer, [Pb(mu-NO2)(mu-pyc)(H2O)](n) (1). Hpyc = 2-pyridine-carboxylic acid] was prepared and characterized by elemental analyses, powder XRD diffraction and IR spectroscopy. Compound 1 was structurally characterized by single-crystal X-ray diffraction and one-dimensional coordination polymer with coordination environment of PbNO6. The thermal stability of compound 1 showed that compound 1 decomposes at 110-500 degrees C and the final product is PbO. This polymeric precursor has been used to make PbO nano-particles using two different surfactants. The new nano-structure was characterized by scanning electron microscopy and X-ray powder diffraction. This study demonstrates that the coordination polymers may be suitable precursors for the preparation of nanoscale materials.eninfo:eu-repo/semantics/closedAccessCrystal structureThermal propertiesNano-materialsCoordination reactionsDiffractionLeadLead oxideMaterials propertiesNanoparticlesScanning electron microscopySurface active agentsThermodynamic stabilityX ray diffractionX ray powder diffractionCoordination environmentCoordination polymersElemental analysisIR spectroscopyNano-materialsNano-scale materialsOne-dimensional coordination polymerPolymeric precursorsPowder XRDSingle crystal x-ray diffractionThermal propertiesThermal stabilityArticle0002761901000052-s2.0-76849101386810813647Materials science, multidisciplinaryPhysics, appliedMetal-Organic Frameworks; X-Ray Powder Diffraction; Elemental Analyses